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Reactions were carried out in a planetary ball mill (Retsch PM100 High Speed Planetary Ball Mill), using a 50 mL stainless steel jar and mix of stainless-steel balls (m = 44.1 g, in which ø = 5 mm, m = 28.1 g and 550 ø = 1–1.2 mm, m = 16.0 g) at 650 rpm for various time periods. The rotation direction was changed every 15 min (3 min during ...

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This video features the SPEX® Mixer/Mill 8000 series and shows how they can prepare tough samples for XRF or ICP Analysis.The 8000D Mixer/Mill is a high-ene...