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Both ranitidine hydrochloride form 1 and form 2 were milled separately in an oscillatory ball mill (Mixer Mill MM301, Retsch & Co., Germany) at 30 Hz. A 1 g powder sample was placed in a 25 mL volume stainless steel milling jar containing two 12 mm diameter stainless steel balls.

Operating Instructions Mixer Mill Type MM 301 Retsch & Co. KG, 42781 Haan, Rheinische Str.36, Germany, Doc.no. D 98.741.9999

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Both ranitidine hydrochloride form 1 and form 2 were milled separately in an oscillatory ball mill (Mixer Mill MM301, Retsch & Co., Germany). A fresh 1 g batch of powder was used for each milling. The powder sample was placed in a 25 mL volume stainless steel milling jar containing two 12 mm diameter stainless steel balls.

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Retsch & Co. KG Rheinische Straße 36 42781 Haan, Germany Telephone +49 2129/5561-0 Telefax +49 2129/8702 E-mail [email protected] Internet Printed in Germany Subject to technical modification 99.741.0001/E-03-2003

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